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Sample text

MS/MS experiments are easy to set up on triple quadrupoles, and are especially valuable when examining complex mixtures of ions. For the coordination/organometallic chemist this is an enormously valuable facility; to a large extent it obviates the need for chromatography and allows analysis of, for example, a reaction mixture directly. Each ion may be selected and individually fragmented to provide structural information exclusively on that ion, without any need for consideration of interference from other ions in the mixture.

QIT/ FTICR machines can store, fragment and deliver controlled quantities of ions for more detailed study in the FTICR cell, and similar advantages are inherent in the QIT/TOF design. 9 (Plate 1) ESI-MSn spectra of [Ru6C(CO)17] in MeOH/NaOMe solution. 2 Summary Strengths       High sensitivity; Multi-stage mass spectrometry (analogous to FTICR experiments); Compact – the smallest mass analysers9; Relatively inexpensive; Robust; Operate at much higher pressure than most mass analysers, so the vacuum system does not need to be as efficient;  Versatile – can be configured with any other mass analyser in useful hybrid instruments.

The depleted lithium, predominantly 7Li, was sold on and this had a noticeable effect on the atomic weight of some supplies of lithium. 2 Isotope Pattern Matching Comparisons between theoretical and experimental isotope patterns are often done by eye, but a direct comparison is highly recommended. This approach enables direct matching between each member of the isotope pattern. 17). 1 m/z, but the match between experimental and calculated patterns is good. In cases as clear-cut as this one, assignment made be made with confidence.

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Ancient Blacksmith, the Iron Age, Damascuc Steel, and Modern Metallurgy


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